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the dissolved solution through filter paper in a funnel into a jar until the
liquid that pours through is clear. The charcoal and sulfur in black powder
are insoluble in water, and so when the solution of water is allowed to
evaporate, potassium nitrate will be left in the jar.
2.32 SULFURIC ACID
Sulfuric acid is far too difficult to make outside of a laboratory or
industrial plant. However, it is readily available in an uncharged car battery.
A person wishing to make sulfuric acid would simply remove the top of a car
battery and pour the acid into a glass container. There would probably be
pieces of lead from the battery in the acid which would have to be removed,
either by boiling or filtration. The concentration of the sulfuric acid can
also be increased by boiling it; very pure sulfuric acid pours slightly faster
than clean motor oil.
2.33 AMMONIUM NITRATE
Ammonium nitrate is a very powerful but insensitive high-order
explosive. It could be made very easily by pouring nitric acid into a large
flask in an ice bath. Then, by simply pouring household ammonia into the flask
and running away, ammonium nitrate would be formed. After the materials have
stopped reacting, one would simply have to leave the solution in a warm place
until all of the water and any unneutralized ammonia or acid have evaporated.
There would be a fine powder formed, which would be ammonium nitrate. It must
be kept in an airtight container, because of its tendency to pick up water from
the air. The crystals formed in the above process would have to be heated VERY
gently to drive off the remaining water.
3.0 EXPLOSIVE RECIPES
Once again, persons reading this material MUST NEVER ATTEMPT TO PRODUCE
ANY OF THE EXPLOSIVES DESCRIBED HEREIN. IT IS ILLEGAL AND EXTREMELY DANGEROUS
TO ATTEMPT TO DO SO. LOSS OF LIFE AND/OR LIMB COULD EASILY OCCUR AS A RESULT
OF ATTEMPTING TO PRODUCE EXPLOSIVE MATERIALS.
These recipes are theoretically correct, meaning that an individual
could conceivably produce the materials described. The methods here are usually
scaled-down industrial procedures.
3.01 EXPLOSIVE THEORY
An explosive is any material that, when ignited by heat or shock,
undergoes rapid decomposition or oxidation. This process releases energy that
is stored in the material in the form of heat and light, or by breaking down
into gaseous compounds that occupy a much larger volume that the original piece
of material. Because this expansion is very rapid, large volumes of air are
displaced by the expanding gasses. This expansion occurs at a speed greater
than the speed of sound, and so a sonic boom occurs. This explains the
mechanics behind an explosion. Explosives occur in several forms: high-order
explosives which detonate, low order explosives, which burn, and primers, which
may do both.
High order explosives detonate. A detonation occurs only in a high
order explosive. Detonations are usually incurred by a shockwave that passes
through a block of the high explosive material. The shockwave breaks apart
the molecular bonds between the atoms of the substance, at a rate approximately
equal to the speed of sound traveling through that material. In a high
explosive, the fuel and oxodizer are chemically bonded, and the shockwave breaks
apart these bonds, and re-combines the two materials to produce mostly gasses.
T.N.T., ammonium nitrate, and R.D.X. are examples of high order explosives.
Low order explosives do not detonate; they burn, or undergo oxidation.
when heated, the fuel(s) and oxodizer(s) combine to produce heat, light, and
gaseous products. Some low order materials burn at about the same speed under
pressure as they do in the open, such as blackpowder. Others, such as gunpowder,
which is correctly called nitrocellulose, burn much faster and hotter when they
are in a confined space, such as the barrel of a firearm; they usually burn
much slower than blackpowder when they are ignited in unpressurized conditions.
Black powder, nitrocellulose, and flash powder are good examples of low order
explosives.
Primers are peculiarities to the explosive field. Some of them, such as
mercury filminate, will function as a low or high order explosive. They are
usually more sensitive to friction, heat, or shock, than the high or low
explosives. Most primers perform like a high order explosive, except that they
are much more sensitive. Still others merely burn, but when they are confined,
they burn at a great rate and with a large expansion of gasses and a shockwave.
Primers are usually used in a small amount to initiate, or cause to decompose,
a high order explosive, as in an artillery shell. But, they are also frequently
used to ignite a low order explosive; the gunpowder in a bullet is ignited by
the detonation of its primer.
3.1 IMPACT EXPLOSIVES
Impact explosives are often used as primers. Of the ones discussed
here, only mercury fulminate and nitroglycerine are real explosives; Ammonium
triiodide crystals decompose upon impact, but they release little heat and no
light. Impact explosives are always treated with the greatest care, and even
the stupidest anarchist never stores them near any high or low explosives.
3.11 AMMONIUM TRIIODIDE CRYSTALS
Ammonium triiodide crystals are foul-smelling purple colored crystals
that decompose under the slightest amount of heat, friction, or shock, if they
are made with the purest ammonia (ammonium hydroxide) and iodine. Such
crystals are said to detonate when a fly lands on them, or when an ant walks
across them. Household ammonia, however, has enough impurities, such as soaps
and abrasive agents, so that the crystals will detonate when thrown,crushed, or
heated. Upon detonation, a loud report is heard, and a cloud of purple iodine
gas appears about the detonation site. Whatever the unfortunate surface that
the crystal was detonated upon will usually be ruined, as some of the iodine
in the crystal is thrown about in a solid form, and iodine is corrosive. It
leaves nasty, ugly, permanent brownish-purple stains on whatever it contacts.
Iodine gas is also bad news, since it can damage lungs, and it settles to the
ground and stains things there also. Touching iodine leaves brown stains on
the skin that last for about a week, unless they are immediately and vigorously
washed off. While such a compound would have little use to a serious terrorist,
a vandal could utilize them in damaging property. Or, a terrorist could throw
several of them into a crowd as a distraction, an action which would possibly
injure a few people, but frighten almost anyone, since a small crystal that
not be seen when thrown produces a rather loud explosion. Ammonium triiodide
crystals could be produced in the following manner:
Materials Equipment
_________ _________
iodine crystals funnel and filter paper
paper towels
clear ammonia
(ammonium hydroxide, two throw-away glass jars
for the suicidal)
1) Place about two teaspoons of iodine into one of the glass jars. The jars
must both be throw away because they will never be clean again.
2) Add enough ammonia to completely cover the iodine.
3) Place the funnel into the other jar, and put the filter paper in the funnel.
The technique for putting filter paper in a funnel is taught in every basic
chemistry lab class: fold the circular paper in half, so that a semi-circle
is formed. Then, fold it in half again to form a triangle with one curved
side. Pull one thickness of paper out to form a cone, and place the cone
into the funnel.
4) After allowing the iodine to soak in the ammonia for a while, pour the
solution into the paper in the funnel through the filter paper.
5) While the solution is being filtered, put more ammonia into the first jar
to wash any remaining crystals into the funnel as soon as it drains.
6) Collect all the purplish crystals without touching the brown filter paper,
and place them on the paper towels to dry for about an hour. Make sure that
they are not too close to any lights or other sources of heat, as they could
well detonate. While they are still wet, divide the wet material into about
eight chunks.
7) After they dry, gently place the crystals onto a one square inch piece of
duct tape. Cover it with a similar piece, and gently press the duct tape
together around the crystal, making sure not to press the crystal itself.
Finally, cut away most of the excess duct tape with a pair of scissors, and
store the crystals in a cool dry safe place. They have a shelf life of
about a week, and they should be stored in individual containers that can be
thrown away, since they have a tendency to slowly decompose, a process which
gives off iodine vapors, which will stain whatever they settle on. One
possible way to increase their shelf life is to store them in airtight
containers. To use them, simply throw them against any surface or place them
where they will be stepped on or crushed.
3.12 MERCURY FULMINATE
Mercury fulminate is perhaps one of the oldest known initiating
compounds. It can be detonated by either heat or shock, which would make it
of infinite value to a terrorist. Even the action of dropping a crystal of
the fulminate causes it to explode. A person making this material would
probably use the following procedure:
MATERIALS EQUIPMENT
_________ _________
mercury (5 g) glass stirring rod
concentrated nitric 100 ml beaker (2)
acid (35 ml)
adjustable heat source
ethyl alcohol (30 ml)
distilled water blue litmus paper
funnel and filter paper
1) In one beaker, mix 5 g of mercury with 35 ml of concentrated nitric acid,
using the glass rod.
2) Slowly heat the mixture until the mercury is dissolved, which is when the
solution turns green and boils.
3) Place 30 ml of ethyl alcohol into the second beaker, and slowly and carefully
add all of the contents of the first beaker to it. Red and/or brown fumes
should appear. These fumes are toxic and flammable.
4) After thirty to forty minutes, the fumes should turn white, indicating that
the reaction is near completion. After ten more minutes, add 30 ml of the
distilled water to the solution.
5) Carefully filter out the crystals of mercury fulminate from the liquid
solution. Dispose of the solution in a safe place, as it is corrosive
and toxic.
6) Wash the crystals several times in distilled water to remove as much excess
acid as possible. Test the crystals with the litmus paper until they are
neutral. This will be when the litmus paper stays blue when it touches the
wet crystals
7) Allow the crystals to dry, and store them in a safe place, far away from
any explosive or flammable material.
This procedure can also be done by volume, if the available mercury
cannot be weighed. Simply use 10 volumes of nitric acid and 10 volumes of
ethanol to every one volume of mercury.
3.13 NITROGLYCERINE
Nitroglycerine is one of the most sensitive explosives, if it is not
the most sensitive. Although it is possible to make it safely, it is difficult.
Many a young anarchist has been killed or seriously injured while trying to
make the stuff. When Nobel's factories make it, many people were killed by the
all-to-frequent factory explosions. Usually, as soon as it is made, it is
converted into a safer substance, such as dynamite. An idiot who attempts
to make nitroglycerine would use the following procedure:
MATERIAL EQUIPMENT
________ _________
distilled water eye-dropper
table salt 100 ml beaker
sodium bicarbonate 200-300 ml beakers (2)
concentrated nitric ice bath container
acid (13 ml) ( a plastic bucket serves well )
concentrated sulfuric centigrade thermometer
acid (39 ml)
glycerine blue litmus paper
1) Place 150 ml of distilled water into one of the 200-300 ml beakers.
2) In the other 200-300 ml beaker, place 150 ml of distilled water and about
a spoonful of sodium bicarbonate, and stir them until the sodium bicarbonate
dissolves. Do not put so much sodium bicarbonate in the water so that some
remains undissolved.
3) Create an ice bath by half filling the ice bath container with ice, and
adding table salt. This will cause the ice to melt, lowering the overall
temperature.
4) Place the 100 ml beaker into the ice bath, and pour the 13 ml of concentrated
nitric acid into the 100 ml beaker. Be sure that the beaker will not spill
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